Quality materials characterization always begins with proper sample preparation. All too often individuals rush to analyze a sample without considering how its intrinsic state will influence results. Considering sample roughness, thickness, critical feature size, or potential sources of contamination are just a few questions to ponder before jumping on that fancy analytical instrument. The MCL has revamped its sample preparation laboratory with new expertise, equipment, and procedures. I will highlight how to get started using this lab and provide general tips & tricks to improve the rigor and reproducibility of your work.